# Summary report for Directory: home/alank/data/reg1103

Report generated Nov 12, 2003; 16:28:29

## Unit cell

6846 reflections with 1.00°<theta<27.10° (resolution between 20.36A and 0.78A) were used for unit cell refinement

Symmetry used in scalepack | p2
a (Angstrom) | 12.6994 +/- 0.0005
b (Angstrom) | 17.2400 +/- 0.0007
c (Angstrom) | 14.8768 +/- 0.0005
alpha (°) | 90.000
beta (°) | 108.853 +/- 0.002
gamma (°) | 90.000
Volume (A**3) | 3082.3 +/- 0.2
Mosaicity (°) | 0.976 +/- 0.002

## Data collection

### Summary

Total number of images collected | 267
Total exposure time | 211.5 minutes
Data collection exposure time | 206.5 minutes
Data collection wall-clock time | 232.6 minutes

### Experimental Conditions

Wavelength | 0.71073 A
Cryostat setting | 123.00K
Generator setting | 55kV 32mA
Crystal to detector distance | 40.00 mm

### Scans

Type | Name | # images | Total Rotation | Per frame Rotation | Exposure per frame | Used in scaling
--- | --- | --- | --- | --- | --- | ---
cell determination | i01f | 10 | `10.0`° omega | 1.000° | 30 seconds | No
data collection | s01f | 180 | `288.0`° phi | 1.600° | 48 seconds | Yes
data collection | s02f | 77 | `123.2`° omega | 1.600° | 48 seconds | Yes

## Scalepack Scaling

### Deleted observations

Rejected | `89`
Zero sigma or profile test | `1`
Overload or incomplete profile | `2114`
Sigma cutoff | `47`
High resolution limit | `110`

### Final Data Set

Scale factor range | 10.00-13.34
Number of 'full' reflections | `7678`
Number of 'partial' reflections | `23849`
Total number of integrated reflections | `29534`
Total number of unique reflections | `7002`
Data completeness | `99.9%`
Resolution range | 20.36-0.78 A
Theta range | 1.00°-27.10°
Average Intensity | `35.4`
Average Sigma(I) | `2.3`
Overall R-merge (linear) | `0.080`