Symmetry used in scalepack | p1 |
---|---|
a (Angstrom) | 11.5255 +/- 0.0009 |
b (Angstrom) | 15.1738 +/- 0.0012 |
c (Angstrom) | 17.7948 +/- 0.0012 |
alpha (°) | 93.900 +/- 0.005 |
beta (°) | 98.116 +/- 0.005 |
gamma (°) | 95.012 +/- 0.004 |
Volume (A**3) | 3058.9 +/- 0.4 |
Mosaicity (°) | 1.750 +/- 0.002 |
Total number of images collected | 1218 |
---|---|
Total exposure time | 16.3 hours |
Data collection exposure time | 16.2 hours |
Data collection wall-clock time | 18.1 hours |
Wavelength | 0.71073 A |
---|---|
Cryostat setting | 123.00K |
Generator setting | 55kV 32mA |
Type | Name | # images | Total Rotation | Per frame Rotation | Exposure per frame | Detector distance | Used in scaling |
---|---|---|---|---|---|---|---|
cell determination | i01f | 10 | 10.0° omega | 1.000° | 40 seconds | 40.00 mm | No |
data collection | s01f | 605 | 363.0° phi | 0.600° | 48 seconds | 39.80 mm | Yes |
data collection | s02f | 64 | 38.4° omega | 0.600° | 48 seconds | 39.80 mm | Yes |
data collection | s03f | 64 | 38.4° omega | 0.600° | 48 seconds | 39.80 mm | Yes |
data collection | s04f | 97 | 58.2° omega | 0.600° | 48 seconds | 39.80 mm | Yes |
data collection | s05f | 97 | 58.2° omega | 0.600° | 48 seconds | 39.80 mm | Yes |
data collection | s06f | 134 | 80.4° omega | 0.600° | 48 seconds | 39.80 mm | Yes |
data collection | s07f | 147 | 88.2° omega | 0.600° | 48 seconds | 39.80 mm | Yes |
Rejected | 235 |
---|---|
Zero sigma or profile test | 120 |
Overload or incomplete profile | 2774 |
Sigma cutoff | 121 |
High resolution limit | 5 |
Scale factor range | 8.97-18.29 |
---|---|
Number of 'full' reflections | 0 |
Number of 'partial' reflections | 42332 |
Total number of integrated reflections | 32623 |
Total number of unique reflections | 10544 |
Data completeness | 96.2% |
Resolution range | 49.66-0.84 A |
Theta range | 0.41°-25.03° |
Average Intensity | 10.3 |
Average Sigma(I) | 2.1 |
Overall R-merge (linear) | 0.163 |